Supra-Clean and Supra-Poly Solid Phase Extraction (SPE

preparation would be if your Solid Phase Extraction (SPE) solutions were precisely manufactured for guaranteed reproducibility. ... Supra-Clean Phenyl...

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Supra-Clean® and Supra-Poly® Solid Phase Extraction (SPE) Solutions

Imagine how much faster, easier and more efficient your sample preparation would be if your Solid Phase Extraction (SPE) solutions were precisely manufactured for guaranteed reproducibility. Not just column to column. Not just batch to batch. But lot to lot—no matter how many days, weeks or years between production times. That’s exactly the kind of confidence and convenience you can expect with the innovative line of Supra-Clean™ silica-based and Supra-Poly™ polymer-based SPE cartridges and columns from PerkinElmer. Our Precise-Bed Technology™ provides precision and manufacturing tolerances of + – 1%, ensuring guaranteed repeatability and optimized recovery reproducibility. The distribution and size of particles is controlled through stringent manufacturing processes, and each finished product is delivered with an individual quality certificate. Experience the difference for yourself. Or—to be more exact— experience the uniformity.

PerkinElmer’s homogeneous filling and mono-dispersed spherical media not only provide unparalleled reproducibility, they also deliver superior performance. Sample diffusion through the media is better than in other systems, improving flow efficiency and avoiding channeling and clogging due to fines. This enables smaller sample sizes to be used without compromising recovery levels, dramatically reducing solvent volumes, analytical costs and processing times.

18

V1

6

With PerkinElmer SPE solutions, you can work faster and more costeffectively, all while experiencing the complete recovery, reproducibility and reliability you need for consistently excellent results.

V2 IR60-40/63SI

0

SPE Supra-Clean 60-50SI

2

V1 < V2 4

6

PerkinElmer’s smaller, more homogeneous, spherical media deliver sharper, narrower peaks for faster, more accurate sample analysis.

2

Spherical media and consistent particle distribution enable smaller elution volumes and better, more reproducible extraction purification, concentration and recovery.

The unsurpassed reproducibility of SPE solutions is the result of a unique bed-packing technique and spherical media. Columns are evenly and consistently filled with particles sized for optimum distribution, delivering a level of performance unattainable with the irregularly shaped silica used in competitive solutions.

250 x 4.6 mm column Hexane - IsoPropanol (97/3) Flow rate: 1.0 ml/min PSI: 1 bars UV: 254 nm A- Tri-Terbutylbenzene B- Diethyl Phthalate

12

Competitor SPE Column

Consistently. Excellent. Performance.

Performance Comparison of PerkinElmer Spherical SPE Media vs. Leading Irregular SPE Silica.

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SPE Column

Answering Your Needs. Empowering Your Lab. Ideal for a broad array of analytes and matrices, SPE solutions are available in a variety of formats including Large Reservoir Capacity (LRC) columns, Polypropylene (PP) columns and cartridges, 96 well plate format, and glass columns. Each technology is offered with a wide selection of polymer and silica sorbents. Varied column capacities and bed weights allow you to perform scalable analyses depending upon your required detection limits.

Choose the Best SPE Solution For Your Method To find the ideal SPE column for your particular application, simply follow the flow diagram below, selecting your path based on the options at each junction.

Your Sample

Type of Matrix

Aqueous

Analyte Solubility

Water

Analyte

Analyte Polarity

Polar

Ionic

Neutral

Neutral

Anionic Acids

Ion Exchange Chromatography

Non-Polar

Reversed Phase Chromatography

Non-Polar

Polar

Normal Phase Chromatography

Supra-Clean Florisil (FL-S) Supra-Clean Silica (SI-S) Supra-Clean Amino (NH2-S) Supra-Clean Polyamine (P6)

Supra-Clean Amino (NH2-S) Supra-Poly 1200 m2/g (XWP)* Supra-Poly (ATH, ATL, AEV)* Supra-Poly HLB

Supra-Clean C18 Supra-Clean 300Å C4 Supra-Clean Phenyl (PH-S) Supra-Clean Cyano (CN-S) Supra-Poly Extreme Capacity 1500 m2/g (XC)* Supra-Poly HLB

Supra-Clean Strong Anion Exchange (SAX) Supra-Clean Amino (NH2-S) Supra-Clean Mixed-Mode (MM1) Supra-Clean Mixed-Mode (MM2)

SPE Strong Cation Exchange (SCX) SPE Weak Cation Exchange (WCX) Supra-Clean Mixed-Mode (MM3)

Supra-Clean REC18

Supra-Clean REC18

Supra-Clean C18 Supra-Clean 300Å C4 Supra-Clean Phenyl (PH-S) Supra-Clean LCC

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Organic Solvents

Cationic Bases

Reversed Phase Chromatography

*AEV = Advanced Environmental ATH = Hydrophobic/Hydrophilic ATL = Lipophilic

Water

path as Ionic analyte)

Moderately Polar

Non-Polar

Follow same path as Organic

Ionic (Follow same

Neutral

Recommended Chromatography

Recommended SPE Products

Organic

HLB = Hydrophilic Lipophylic Balanced XC = Extreme Capacity XWP = Extra Wide Particle

3

A WIDE ARRAY OF

COLUMNS FOR A

BROAD RANGE OF

APPLICATIONS

SUPRA-CLEAN SPHERICAL SILICA

Phase Mechanism Interaction mode Compounds Matrix C18-S Hydrophobic Reversed Phase Polar to Non-Polar compounds Biological fluids, aqueous samples High Recovery REC18 Hydrophobic Reversed Phase Non-polar and mid-polar compounds Biological fluids, aqueous samples including 100% water solvents Phenyl (PH-S) Hydrophobic Reversed Phase

Non-polar to mid-polar Biological fluids aromatic compounds

Silica (SI-S) Hydrophilic Normal Phase Polar compounds Non-polar organics, oils, lipids Amino (NH2-S) Hydrophilic Normal Phase

Polar to Mid-Polar aromatic compounds

Biological fluids, aqueous samples, buffered organics

Strong Cation Ion Exchange Ion Exchange Basic compounds Biological fluids, aqueous samples, Exchange (SCX) buffered organics Weak cation Ion Exchange Ion Exchange Strong basic compounds Biological fluids, aqueous samples Exchange (WCX) Strong Anion Ion Exchange Ion Exchange Acidic compounds Biological fluids, aqueous samples Exchange (SAX) Cyano (CN-S)

Hydrophilic

Normal Phase

Polar to Mid-Polar compounds

Non-polar organics, oils, lipids

Florisil (FL-S) Hydrophilic Normal Phase Polar compounds Ideal for polar compounds in non-polar matrix

Florisil Pesticide (FL-S) Hydrophilic Normal Phase Polar compounds Ideal for polar compounds in non-polar matrix Polyamine (P6) Hydrophilic Reversed Phase

Carboxylic acids, phenolics Aqueous and mid-polar matrices and nitroaromatics

300 A (C4)

Hydrophobic

Reversed Phase

Non-polar to mid-polar compounds

Biological Samples

LCC

Hydrophobic

Reversed Phase

Non-polar to mid-polar compounds

Biological fluids, aqueous samples

Mixed mode (MM1)

Ion Exchange/ Hydrophobic

Reversed Phase / SCX

Basic compounds

Biological samples

Mixed mode (MM2)

Ion Exchange/ Hydrophobic

Reversed Phase / WCX

Very basic compounds

Biological samples

Mixed mode (MM3)

Ion Exchange/ Hydrophobic

Reversed Phase / SAX

Acidic compounds

Biological samples

SUPRA-POLY SPHERICAL POLYMER Extreme Capacity (XC)

Hydrophobic

Reversed Phase

Polar and non-polar

Aqueous or organic

Extreme Capacity Hydrophobic Reversed Phase Polar and non-polar Biological and viscous samples Wide Pore (XWP) Hydrophilic (ATH) Hydrophilic Reversed Phase Mid to non-polar compounds Aqueous or organic

Lipophilic (ATL) Lipophilic Reversed Phase Mid to non-polar compounds Crude samples Environmental (AEV) Hydrophilic/ Hydrophobic Reversed Phase Mid to non-polar compounds Aqueous or Organic HLB Hydrophilic/lipophilic balanced Reversed Phase Mid to non-polar compounds Aqueous or organic

4



Typical Applications Drugs and drug metabolites in biological matrices, trace organic material in water, toxins in food

pH Range

End- capping

Pore Size (A)

Surface Area (m2/g)

Particle Size (um)

2-8

Yes

60

500

50

Comments 18% Carbon Load (CL)

Drugs and drug metabolites in biological 2-8 Yes NA NA 50 matrices, trace organic material in water, toxins in food

High capacity and better recovery especially for high acqueous conditions. 15% CL

Benzodiazepines in biological matrices, extraction of aromatic compounds

2-8

No

60

500

50

9% CL

Aldehydes, amines, pesticides, herbicides, carotenoids, fat soluable vitamins, baflatoxins, fatty acids, and phospholipids

2-8

No

60

500

50

Bare Silica

Basic compounds, polar amine compounds, carbohydrates

2-8

No

60

500

50

5% CL

Cations, antibiotics, drugs, amino acids, 2-8 No 60 450 60 catecholamines, herbicides, nucleic acid bases, nucleosides, and surfactants

Strong Acid - Sulfonic acid; Exchange capacity 0.70 meq/g

Cations, amines, antibiotics, drugs, amino acids, 2-8 No 60 450 60 Weak Acid - Carboxylic acid; Exchange catecholamines, nucleic acid bases, nucleosides, capacity 0.22 meq/g and surfactants Acidic food pigments, organic acids, phenol 2-8 No 60 450 60 compounds, nucleic acids, nucleotides, surfactants Polar compounds in hexane and oil

2-8

Yes

60

500

50

Strong Base - quaternary amine; Exchange capacity 0.30 meq/g 8% CL; Mid-range polarity between silica and C18

Pesticides, Polychlorinated Biphenyls (PCB) 2-8 No NA NA 200

Standard grade. Alternative to silica for viscous matrices due to large particle size.

Pesticides 2-8 No NA NA 200

High purity pesticide grade. Alternative to silica for viscous matrices

Aromatic and naturalproducts; Flavones, Chalkones, Anthraquinones

2-8

No

NA

Hydrophobic peptides and polypeptides Non-polar compounds in aqueous solution

NA

100

Nylon 6

2-8

No

300

-

-

Large pore size for isolation of large biomolecules

2-8

Yes

60

500

50

10% CL; Lower carbon load than C18-S and REC18

Drugs and drug metabolites

2-8

No

60

450

60

Exchange capacity 0.09 meq/g

Drugs and drug metabolites

2-8

No

60

450

60

Exchange capacity 0.10 meq/g

Drugs and drug metabolites

2-8

No

60

450

60

Exchange capacity 0.14 meq/g

Drugs and drug metabolites biological fluids

0-14

No

NA

1500

70

Drugs and drug metabolites biological fluids 0-14 No Wide Pore 1200 90 Mid-polar and non-polar compounds in aqueous and organic solvents

1-13

No

70

800

75

Lipids 0-14 No 70 800 100

High capacity polystyrene-divinylbenzene (PSDVB) High capacity PSDVB for large biomolecules and viscous matrices Mixed hydrophilic/hydrophobic interactions PSDVB; Alternative to high flow silica for mid-polar to non-polar compounds (<3000D) in crude samples

Aqueous environmental compounds that are 1-12 No 70 800 75 not retained on C18

Advanced environmental; Polystyrene-co-2hydroxyethyl methacrylate (PSHEMA)

Mid-polar and non-polar compounds in 0-14 No 80 850 30 & 60 aqueous and organic solvents

Hydrophilic-lipophilic-balanced reversedphase sorbent for acids, bases and neutrals

www.perkinelmer.com/spe

5

PerkinElmer offers a comprehensive selection of SPE products that have been precisely manufactured for guaranteed reproducibility. Not just column to column. Not just batch to batch. But lot to lot — no matter how many days, weeks or years between production times. Supra-Clean and Supra-Poly SPE products are available in a range of media weights, volumes and formats, including easy to order selection kits and application packs.

SUPRA-CLEAN COLUMNS AND 96 WELL PLATES • Pure spherical silica • Pore size 60 - 120 Å • 20 chemistries with pH range 2-8

Supra-Clean C18

Supra-Clean REC18

Columns

Columns

Media Weight

Volume

Part No.

Quantity

Media Weight

Volume

Part No.

Quantity

50 mg

1 ml

N9306476

50

50 mg

1 ml

N9306519

50

100 mg

1 ml

N9306478

100

100 mg

1 ml

N9306520

100

100 mg

3 ml

N9306523

50

100 mg

3 ml

N9306455

50

3 ml

N9306521

50

200 mg

3 ml

N9306462

50

200 mg

500 mg

3 ml

N9306438

50

500 mg

3 ml

N9306522

50

6 ml

N9306633

30

500 mg

3 ml*

N9306642

50

200 mg

200 mg

6 ml

N9306634

30

500 mg

6 ml

N9306457

30

6 ml

N9306491

30

Volume

Part No.

Quantity

500 mg

6 ml

N9306448

30

1g

500 mg

6 ml*

N9306640

30

96 Well Plates

1g

6 ml

N9306422

30

2g

6 ml

N9306430

30

2g

15 ml

N9306479

20

2g

25 ml

N9306475

20

Media Weight

25 mg

2 ml

N9306563

1

50 mg

2 ml

N9306564

1

100 mg

2 ml

N9306565

1

* Not end-capped

Supra-Clean Strong Anion Exchange (SAX)

96 Well Plates Media Weight

Volume

Part No.

Quantity

Columns

25 mg

2 ml

N9306566

1

Media Weight

Volume

Part No.

Quantity

50 mg

2 ml

N9306567

1

50 mg

1 ml

N9306553

50

100 mg

2 ml

N9306568

1

100 mg

1 ml

N9306471

100

100 mg

3 ml

N9306554

50

Supra-Clean C18 Cartridges Media Weight

Volume

Part No.

Quantity

390 mg

--

N9306587

50

910 mg

--

N9306588

50

1690 mg

--

N9306589

50

200 mg

3 ml

N9306482

50

500 mg

3 ml

N9306555

50

500 mg

6 ml

N9306556

30

Volume

Part No.

Quantity

96 Well Plates Media Weight

6

25 mg

2 ml

N9306581

1

50 mg

2 ml

N9306582

1

100 mg

2 ml

N9306583

1

Supra-Clean 300Å C4 96 Well Plates

Columns Media Weight

Volume

Part No.

Quantity

50 mg

1 ml

N9306590

50

100 mg

1 ml

N9306591

100

100 mg

3 ml

N9306592

50

200 mg

3 ml

N9306593

50

Media Weight

Volume

Part No.

Quantity

25 mg

2 ml

N9306578

1

50 mg

2 ml

N9306579

1

100 mg

2 ml

N9306580

1

Supra-Clean Mixed-Mode (MM2) Columns

Supra-Clean Strong Cation Exchange (SCX) Columns Media Weight

Volume

Part No.

Quantity

50 mg

1 ml

N9306536

50

100 mg

1 ml

N9306432

100

100 mg

3 ml

N9306537

50

200 mg

3 ml

N9306538

50

500 mg

3 ml

N9306539

50

500 mg

6 ml

N9306540

30

Media Weight

Volume

Part No.

Quantity

25 mg

2 ml

N9306575

1

50 mg

2 ml

N9306576

1

100 mg

2 ml

N9306577

1

96 Well Plates

Media Weight

Volume

Part No.

Quantity

50 mg

1 ml

N9306548

50

100 mg

1 ml

N9306549

100

100 mg

3 ml

N9306550

50

200 mg

3 ml

N9306551

50

500 mg

3 ml

N9306411

50

500 mg

6 ml

N9306552

30

Supra-Clean Mixed-Mode (MM3) Columns Media Weight

Volume

Part No.

Quantity

500 mg

6 ml

N9306649

30

Supra-Clean Florisil (FL-S) Columns

Supra-Clean Weak Cation Exchange (WCX) Columns Media Weight

Volume

Part No.

Quantity

50 mg

1 ml

N9306544

50

100 mg

1 ml

N9306545

100

100 mg

3 ml

N9306546

50

200 mg

3 ml

N9306547

50

500 mg

3 ml

N9306420

50

500 mg

6 ml

N9306407

30

Media Weight

Volume

Part No.

Quantity

200 mg

3 ml

N9306511

50

500 mg

3 ml

N9306512

50

500 mg

6 ml

N9306494

30

1g

6 ml

N9306413

30

2g

6 ml

N9306513

20

2g

15 ml

N9306514

20

2g

25 ml

N9306515

20

Supra-Clean Florisil (FL-S) Pesticide Grade

Supra-Clean Mixed-Mode (MM1)

Columns

Columns

Media Weight

Volume

Part No.

Quantity

200 mg

3 ml

N9306516

50

50

500 mg

3 ml

N9306400

50

N9306542

100

500 mg

6 ml

N9306517

30

3 ml

N9306419

50

1g

6 ml

N9306436

30

200 mg

3 ml

N9306543

50

2g

6 ml

N9306470

30

500 mg

3 ml

N9306481

50

2g

15 ml

N9306443

20

500 mg

6 ml

N9306416

30

2g

25 ml

N9306447

20

200 mg

15 ml

N9306713

20

Media Weight

Volume

Part No.

Quantity

50 mg

1 ml

N9306541

100 mg

1 ml

100 mg

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7

Supra-Clean Silica (SI-S)

Supra-Clean Polyamine (P6)

Columns

Columns

Media Weight

Volume

Part No.

Quantity

Media Weight

Volume

Part No.

Quantity

100 mg

3 ml

N9306532

50

500 mg

3 ml

N9306518

50

200 mg

3 ml

N9306444

50

500 mg

6 ml

N9306434

30

500 mg

3 ml

N9306402

50

500 mg

6 ml

N9306466

30

Supra-Clean Phenyl (PH-S)

1g

6 ml

N9306404

30

Columns

2g

6 ml

N9306533

20

2g

15 ml

N9306534

20

2g

25 ml

N9306535

20

Cartridges Media Weight

Volume

Part No.

Quantity

300 mg

--

N9306584

50

Media Weight

Volume

Part No.

Quantity

50 mg

1 ml

N9306401

50

100 mg

1 ml

N9306524

100

100 mg

3 ml

N9306525

50

200 mg

3 ml

N9306490

50

500 mg

3 ml

N9306421

50

6 ml

N9306526

30

6 ml

N9306527

30

700 mg

--

N9306585

50

500 mg

1300 mg

--

N9306586

50

1g 96 Well Plates

Supra-Clean Cyano (CN-S) Columns

Media Weight

Volume

Part No.

Quantity

25 mg

2 ml

N9306569

1

Media Weight

Volume

Part No.

Quantity

50 mg

2 ml

N9306570

1

500 mg

3 ml

N9306645

50

100 mg

2 ml

N9306571

1

500 mg

6 ml

N9306644

30

Supra-Clean LCC Supra-Clean Amino (NH2-S)

Columns

Columns

Media Weight

Volume

Part No.

Quantity

Media Weight

Volume

Part No.

Quantity

500 mg

3 ml

N9306643

50

50 mg

1 ml

N9306528

50

500 mg

6 ml

N9306641

30

100 mg

1 ml

N9306410

100

100 mg

3 ml

N9306529

50

500 mg

3 ml

N9306414

50

200 mg

6 ml

N9306530

50

500 mg

6 ml

N9306531

30

Media Weight

Volume

Part No.

Quantity

96 Well Plates

8

25 mg

2 ml

N9306572

1

50 mg

2 ml

N9306573

1

100 mg

2 ml

N9306574

1

SUPRA-POLY HLB COLUMNS AND 96 WELL PLATES • Contains macro-porous polymers with ultra-pure, pharmaceutical grade spherical particles • Shorter analysis times, greater load capacity and reduced solvent usage • Ideal for high throughput assays

Supra-Poly HLB 30 µm Columns Media Weight

Volume

Part No.

Quantity

30 mg

1 ml

N9306650

50

50 mg

1 ml

N9306655

50

60 mg

1 ml

N9306656

50

100 mg

1 ml

N9306657

50

30 mg

3 ml

N9306651

50

Media Weight

Volume

Part No.

Quantity

200 mg

6 ml*

N9306693

30

500 mg

6 ml

N9306684

30

500 mg

15 ml

N9306685

20

500 mg

6 ml*

N9306694

30

1g

15 ml

N9306686

20

30 mg

15 ml**

N9306688

50

60 mg

15 ml**

N9306689

50

100 mg

15 ml**

N9306690

50

200 mg

15 ml**

N9306691

50

1g

25 ml

N9306687

20

60 mg

3 ml

N9306658

50

100 mg

3 ml

N9306659

50

200 mg

3 ml

N9306660

50

500 mg

3 ml

N9306661

30

100 mg

6 ml*

N9306672

30

150 mg

6 ml

N9306662

30

200 mg

6 ml

N9306663

30

200 mg

6 ml*

N9306673

30

500 mg

6 ml*

N9306674

30

500 mg

6 ml

N9306664

30

500 mg

15 ml

N9306665

20

1g

15 ml

N9306666

20

Media Weight

Volume

30 mg

15 ml**

N9306668

50

30 mg

60 mg

15 ml**

N9306669

50

50 mg

100 mg

15 ml**

N9306670

50

60 mg

200 mg

15 ml**

N9306671

50

1g

25 ml

N9306667

20

Media Weight

Volume

Part No.

Quantity

30 mg

1 ml

N9306652

50

* Glass columns

** LRC columns

30 µm 96 Well Plates Media Weight

Volume

Part No.

Quantity

30 mg

2 ml

N9306698

1

50 mg

2 ml

N9306699

1

60 mg

2 ml

N9306700

1

Part No.

Quantity

2 ml

N9306695

1

2 ml

N9306696

1

2 ml

N9306697

1

60 µm 96 Well Plates

60 µm Columns

50 mg

1 ml

N9306675

50

60 mg

1 ml

N9306676

50

100 mg

1 ml

N9306677

50

30 mg

3 ml

N9306653

50

60 mg

3 ml

N9306678

50

100 mg

3 ml

N9306679

50

200 mg

3 ml

N9306680

50

500 mg

3 ml

N9306681

30

100 mg

6 ml*

N9306692

30

150 mg

6 ml

N9306682

30

200 mg

6 ml

N9306683

30

www.perkinelmer.com/spe

9

SUPRA-POLY COLUMNS AND 96 WELL PLATES • Contains macro-porous polymers with ultra-pure, pharmaceutical grade spherical particles • Shorter analysis times, greater load capacity and reduced solvent usage • Ideal for high throughput assays

Supra-Poly Extreme Capacity 1500 m2/g (XC)

Supra-Poly Environmental (AEV)

Columns

Columns

Media Weight

Volume

Part No.

Quantity

Media Weight

Volume

Part No.

Quantity

30 mg

1 ml

N9306441

50

100 mg

3 ml

N9306648

50

50 mg

1 ml

N9306500

50

60 mg

1 ml

N9306501

50

Supra-Poly Hydrophilic (ATH)

100 mg

1 ml

N9306403

50

Columns

60 mg

3 ml

N9306502

50

100 mg

3 ml

N9306440

50

200 mg

3 ml

N9306428

50

200 mg

6 ml

N9306635

30

500 mg

6 ml

N9306405

30

1g

15 ml

N9306503

20

96 Well Plates

Media Weight

Volume

Part No.

Quantity

100 mg

3 ml

N9306646

50

200 mg

3 ml

N9306638

50

200 mg

6 ml

N9306636

30

Supra-Poly Lipophilic (ATL) Columns

Media Weight

Volume

Part No.

Quantity

30 mg

2 ml

N9306557

1

50 mg

2 ml

N9306558

1

60 mg

2 ml

N9306559

1

Media Weight

Volume

Part No.

Quantity

100 mg

3 ml

N9306647

50

200 mg

3 ml

N9306639

50

200 mg

6 ml

N9306637

30

Supra-Poly Extra Wide Particle 1200 m2/g (XWP) Columns Media Weight

Volume

Part No.

Quantity

30 mg

1 ml

N9306504

50

50 mg

1 ml

N9306427

50

60 mg

1 ml

N9306505

50

100 mg

1 ml

N9306506

50

60 mg

3 ml

N9306507

50

100 mg

3 ml

N9306508

50

200 mg

3 ml

N9306509

50

500 mg

6 ml

N9306418

30

1g

15 ml

N9306510

20

96 Well Plates

10

Media Weight

Volume

Part No.

Quantity

30 mg

2 ml

N9306560

1

50 mg

2 ml

N9306561

1

60 mg

2 ml

N9306562

1

Compared to other industry leading SPE materials, our Extreme Capacity (XC) and Extra Wide Particles (XWP) lead market in surface area. This allows for higher capacities at lower bed weights.

SPE SELECTION KITS: Enables quick column selection for development of reproducible and repeatable SPE methods. Description

Media Weight

Volume

Part No.

Quantity

Pre-Concentration of Hydrophobic Compounds from Aqueous Matrix

200 mg 200 mg

6 ml 3 ml

N9306594 N9306595

50 50

Extraction of Hydrophobic Compounds from Aqueous Matrix

500 mg 500 mg

6 ml 3 ml

N9306596 N9306597

50 50

Pre-Concentration of Hydrophilic Compounds

500 mg 500 mg

6 ml 3 ml

N9306598 N9306599

30 30

Removal of Polar Compounds from Aqueous and Organic Matrix

500 mg 500 mg

6 ml 3 ml

N9306600 N9306601

30 30

Extraction of Acidic Basic and Neutral Compounds from Aqueous or Organic Matrix

100 mg

3 ml

N9306602

50

Extraction of Carboxylic Acids and Strong Bases from Aqueous Matrix

500 mg

6 ml

N9306603

40

Extraction of Weak Bases from Aqueous Matrix

500 mg

6 ml

N9306604

30

SPE APPLICATION PACKS: Ideal for extraction of known entities from a variety of matrices, our packs are expertly tailored to meet your application needs and are designed to support major EPA methods and applications. Description

Media Weight

Volume

Part No.

Quantity

Extraction of Basic Drugs from Biological Fluids

200 mg

3 ml

N9306605

50

Extraction of Bisphenol A from Aqueous Matrix

1g

6 ml

N9306613

30

500 mg 1g

3 ml 6 ml

N9306612 N9306611

50 30

Extraction of PAH from Soil and Oil

1.5 g

6 ml

N9306609

30

Extraction of PAH from Soil and Oil (Glass Straight Column)

1.5 g

6 ml

N9306610

30

Extraction of PAH from Water Containing Humic Acids

1.5 g

6 ml

N9306608

30

Extraction of PAH from Water or Soil

4g

6 ml

N9306606

30

Extraction of PAH from Water or Soil (Glass Straight Column)

4g

6 ml

N9306607

30

Extraction of PCB from Oil

1g 1g

6 ml 3 ml

N9306617 N9306616

30 50

Extraction of Pesticides and Herbicides from Aqueous Matrix

500 mg

3 ml

N9306614

50

Extraction of Steroids from Biological Fluids

500 mg

6 ml

N9306615

30

1g

6 ml

N9306618

30

Extraction of Oil and Grease from Aqueous Matrix-EPA 1664

Extraction of SVOC from Water-EPA 525

SPE VACUUM PUMPS, MANIFOLDS AND ACCESSORIES: SPE Vacuum Manifolds accommodate either 12 or 24 cartridges; 1, 3, 6, 15, and 25 mL columns can be used. Manifolds are equipped with a vacuum port to connect a standard laboratory vacuum pump. Vacuum pulls the sample through the stationary phase, metered by the stopcocks, to control the speed of the extraction process and the sample flow. Waste and wash solvents are discarded and analytes are collected in sample tubes below the manifold completing the extraction. Description

12 Position Part No.

Quantity

24 Position Part No.

Quantity

Vacuum Manifold

N9306619

1 each

N9306626

1 each

Replacement Chamber (Glass)

N9306620

1 each

N9306627

1 each

Cover Gasket - 12 Position

N9306621

1 each

N9306628

1 each

Stopcocks - 12 Position

N9306624

12 pack

N9306631

24 pack

Needles - Polypropylene

N9306622

12 pack

N9306629

24 pack

Needles - Stainless Steel

N9306623

12 pack

N9306630

24 pack

Drying Attachment

N9306625

1 each

N9306632

1 each

Description

Vacuum Pumps

www.perkinelmer.com/spe

20 L/min 115V

60 L/min 115V

17 L/min 230V

58 L/min 230V

Quantity

N9308035

N9308063

N9308331

N9308332

1 each

11

At PerkinElmer, we understand that sample preparation is one of the most critical steps in the analytical process. Often accounting for 60% or more of your timetable, it has a fundamental impact on a wide range of operational parameters. Any errors within this process undermine the quality of your data at all subsequent stages of your analysis. Solid Phase Extraction helps avoid potential errors in sample preparation, reducing re-runs and dramatically increasing productivity. As one of the most cost-effective and flexible tools within the laboratory environment, SPE also provides efficient sample concentration and purification prior to many of today’s most popular analytical techniques, including HPLC, LC/MS, GC and GC/MS.

The right accessories, consumables, methods and application support are as integral to the success of your laboratory as your instrumentation. That’s why we invest heavily in testing and validating our complete portfolio of solutions to ensure you receive accurate, repeatable results on time, every time.

SPE columns are part of PerkinElmer’s complete offering of analytical solutions—an industry-leading portfolio that encompasses instruments, accessories, consumables, supplies, training and service. It’s a breadth of capabilities that enables us to offer the ease and convenience of having a single supplier for all your needs at every stage of your workflow. So you can benefit from greater responsiveness, superior reliability, and dramatic cost savings.

Couple SPE With Leading Instrumentation For Ultimate Laboratory Efficiency Clarus® 680/580/480 GC Clarus SQ 8 GC/MS Flexar™ SQ 300 MS Flexar LC and UHPLC

PerkinElmer, Inc. 940 Winter Street Waltham, MA 02451 USA P: (800) 762-4000 or (+1) 203-925-4602 www.perkinelmer.com

Our OneSource Laboratory Services division even takes it a step further. With more than 1,500 trained and certified field service engineers and service personnel around the world, OneSource offers the most comprehensive portfolio of professional laboratory services in the industry, including complete care programs for virtually every technology and manufacturer. So turn to PerkinElmer. For the experience. For the confidence. For the better.